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Synthesis and crystal structure of 2-chloro-1-(3-hy-droxy-phen-yl)ethanone.

ABSTRACT: The structure of 2-chloro-1-(3-hy-droxy-phen-yl)ethanone, C8H7ClO2, an α-halo-ketone is described. The mol-ecule is planar (r.m.s. deviation = 0.0164 Å) and in the crystal, inversion-symmetric dimers are formed as a result of pairs of strong O-H⋯O and weak C-H⋯O hydrogen bonds. A brief comparison is made with structurally related compounds deposited in the CSD. In addition, the synthesis and some spectroscopic details are presented.

SUBMITTER: Priyanka P 

PROVIDER: S-EPMC9638980 | biostudies-literature | 2022 Nov

REPOSITORIES: biostudies-literature

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Synthesis and crystal structure of 2-chloro-1-(3-hy-droxy-phen-yl)ethanone.

Priyanka Prabhakar P   Jayanna Bidarur K BK   Vinaya   Shankara Prasad Holehundi J HJ   Divakara Thayamma R TR   Yathirajan Hemmige S HS   Parkin Sean S  

Acta crystallographica. Section E, Crystallographic communications 20221020 Pt 11

The structure of 2-chloro-1-(3-hy-droxy-phen-yl)ethanone, C<sub>8</sub>H<sub>7</sub>ClO<sub>2</sub>, an α-halo-ketone is described. The mol-ecule is planar (r.m.s. deviation = 0.0164 Å) and in the crystal, inversion-symmetric dimers are formed as a result of pairs of strong O-H⋯O and weak C-H⋯O hydrogen bonds. A brief comparison is made with structurally related compounds deposited in the CSD. In addition, the synthesis and some spectroscopic details are presented. ...[more]

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