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Visible-Light-Mediated Stadler-Ziegler Arylation of Thiosugars with Anilines.

ABSTRACT: Here, we report a one-pot Stadler-Ziegler reaction toward the synthesis of 1-thioglycosides in good yield from commercially available anilines and (un)protected 1-glycosyl thiols. This simple and mild approach employs the photoredox catalyst [Ru(bpy)3](PF6)2 under visible light.

SUBMITTER: Zhu M 

PROVIDER: S-EPMC9955296 | biostudies-literature | 2022 Aug

REPOSITORIES: biostudies-literature

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Visible-Light-Mediated Stadler-Ziegler Arylation of Thiosugars with Anilines.

Zhu Mingxiang M   Ghouilem Juba J   Messaoudi Samir S  

ACS organic & inorganic Au 20220328 4

Here, we report a one-pot Stadler-Ziegler reaction toward the synthesis of 1-thioglycosides in good yield from commercially available anilines and (un)protected 1-glycosyl thiols. This simple and mild approach employs the photoredox catalyst [Ru(bpy)<sub>3</sub>](PF<sub>6</sub>)<sub>2</sub> under visible light. ...[more]

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