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Low-temperature redetermination of tribenzyl-chloridotin(IV).


ABSTRACT: Compared to the previous studies [Ng (1997 ?). Acta Cryst. C53, 56-58; Yin et al. (2005 ?). Huaxue Shiji, 27, 295-296], the redetermined structure of the title compound, [Sn(C(7)H(7))(3)Cl], exhibits a doubled c unit-cell parameter. There are two mol-ecules in the asymmetric unit, with both Sn and both Cl atoms having 3 site symmetry. The Sn atoms have distorted SnClC(3) tetra-hedral geometries and the mol-ecules inter-act by way of short Sn?Cl bridges [Sn?Cl = 3.418?(2) and 3.475?(2)?Å], thereby forming chains propagating in c.

SUBMITTER: Ng SW 

PROVIDER: S-EPMC2968220 | BioStudies | 2009-01-01T00:00:00Z

REPOSITORIES: biostudies

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