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Crystal structure of 4-[(3-meth-oxy-2-oxidobenzyl-idene)azaniumyl]-benzoic acid methanol monosolvate.

ABSTRACT: In the crystal of the title compound, C15H13NO4·CH3OH, the Schiff base mol-ecule exists in the zwitterionic form; an intra-molecular N-H⋯O hydrogen bond stabilizes the mol-ecular structure. The benzene rings are nearly co-planar, subtending a dihedral angle of 5.34 (2)°. In the crystal, classical O-H⋯O and weak C-H⋯O hydrogen bonds link the Schiff base mol-ecules and methanol solvent mol-ecules into a three-dimensional supra-molecular architecture. The crystal studied was refined as an inversion twin.

SUBMITTER: Kamaal S 

PROVIDER: S-EPMC6281083 | biostudies-literature | 2018 Dec

REPOSITORIES: biostudies-literature

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Crystal structure of 4-[(3-meth-oxy-2-oxidobenzyl-idene)azaniumyl]-benzoic acid methanol monosolvate.

Kamaal Saima S   Faizi Md Serajul Haque MSH   Ali Akram A   Ahmad Musheer M   Iskenderov Turganbay T  

Acta crystallographica. Section E, Crystallographic communications 20181122 Pt 12

In the crystal of the title compound, C<sub>15</sub>H<sub>13</sub>NO<sub>4</sub>·CH<sub>3</sub>OH, the Schiff base mol-ecule exists in the zwitterionic form; an intra-molecular N-H⋯O hydrogen bond stabilizes the mol-ecular structure. The benzene rings are nearly co-planar, subtending a dihedral angle of 5.34 (2)°. In the crystal, classical O-H⋯O and weak C-H⋯O hydrogen bonds link the Schiff base mol-ecules and methanol solvent mol-ecules into a three-dimensional supra-molecular architecture. The  ...[more]

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